The Zilm Laboratory

magnetic resonance for chemistry

Publications

PUBLICATIONS for Kurt W. Zilm:

  1. Pugmire, R. J., Grant, D. M., Zilm, K. W., Anderson, L. L., Oblad, A. G., and Wood, R. E., “13C Magnetic-Resonance of Coal-Derived Liquids”, Fuel, 56, 295 (1977).
  2. Zilm, K. W., Conlin, R. T., Grant, D. M., and Michl, J., “Low-Temperature Natural- Abundance 13C NMR-Spectroscopy of Matrix-Isolated Species: Anisotropy of Shielding Tensor in Ethylene”, Journal of the American Chemical Society, 100, 8038 (1978).
  3. Zilm, K. W., Alderman, D. W., and Grant, D. M., “A High-Speed Magic Angle Spinner”, Journal of Magnetic Resonance, 30, 563 (1978).
  4. Zilm, K. W. and Grant, D. M., “Magic Angle Spinning Without the Magic and Natural Abundance Matrix Isolation 13C NMR” Magnetic Resonance and Related Phenomena, Ed. by E. Kundla, E. Lippma and T. Saluvere, Springer-Verlag Berlin-Heidelberg-New York, 1979, p.98 Proceedings of XXth Congress AMPERE Tallinn, August 21-26, (1978).
  5. Zilm, K. W., Pugmire, R. J., Grant, D. M., Wood, R. E., and Wiser, W. H., “Comparison of the 13C NMR-Spectra of Solid Coals and Their Liquids Obtained By Catalytic- Hydrogenation”, Fuel, 58, 11 (1979).
  6. Zilm, K. W., Conlin, R. T., Grant, D. M., and Michl, J., “Low-Temperature 13C Magnetic-Resonance of Solids I. Alkenes and Cycloalkenes”, Journal of the American Chemical Society, 102, 6672 (1980).
  7. Zilm, K. W., Grant, D. M., Englert, E., and Straight, R. C., “The Use of Solid 13C Nuclear Magnetic Resonance For the Characterization of Cholesterol and Bilirubin Pigment Composition of Human Gallstones”, Biochemical and Biophysical Research Communica- tions, 93, 857 (1980).
  8. Straight, R. C., Zilm, K. W., Englert, E., and Grant, D. M., “The Use of Solid 13C Nuclear Magnetic-Resonance For the Characterization of Cholesterol and Bilirubin Pigment Composition of Human Gallstones”, Gastroenterology, 78, 1271 (1980).
  9. Bunger, J. W., Cogswell, D. E., and Zilm, K. W., “Properties of Asphaltenes From Oil Sand Bitumen and the Effect of Asphaltenes on the Conversion of Bitumens Through Hydropyrolysis”, Erdol & Kohle Erdgas Petrochemie, 34, 179 (1981).
  10. Dalling, D. K., Zilm, K. W., Grant, D. M., Heeschen, W. A., Horton, W. J., and Pugmire, R. J., “A Solution and Solid 13C Magnetic-Resonance Study of the Conformation of 9,10- Dihydroanthracene and its 9,10-Methylated Derivatives”, Journal of the American Chemical Society, 103, 4817 (1981).
  11. Zilm, K. W., and Grant, D. M., “13C Dipolar Spectroscopy of Small Organic-Molecules in Argon Matrices”, Journal of the American Chemical Society, 103, 2913 (1981).
  12. Zilm, K. W., Pugmire, R. J., Larter, S. R., Allan, J., and Grant, D. M., “C-13 CP-MAS Spectroscopy of Coal Macerals”, Fuel, 60, 717 (1981).
  13. Wilson, M. A., Pugmire, R. J., Zilm, K. W., Goh, K. M., Heng, S., and Grant, D. M., “Cross-Polarization 13C NMR Spectroscopy With Magic Angle Spinning Characterizes Organic-Matter in Whole Soils”, Nature, 294, 648 (1981).
  14. Zilm, K. W., Beeler, A. J., Grant, D. M., Michl, J., Chou, T. C., and Allred, E. L., “C-13 Magnetic-Resonance Dipolar Spectroscopy - Orientation of the Chemical-Shift Tensor in Cyclopropane”, Journal of the American Chemical Society, 103, 2119 (1981).

  15. Wilson, M. A., Pugmire, R. J., Vassallo, A. M., Grant, D. M., Collin, P. J., and Zilm, K.W., “Changes in Aromaticity During Coal-Liquefaction”, Industrial & Engineering Chemistry Product Research and Development, 21, 477 (1982).

  16. Pugmire, R. J.; Zilm, K. W.; Woolfenden, W.W.; Grant, D. M.; Dyrkacz, G. R.; Bloom- quist, C. A. A.; Horwitz, E. P., “Carbon-13 Spectra of Macerals Separated from Individual Coals” Organic Geochemistry, 4, 79 (1982).
  17. Zilm, K. W., and Grant, D. M., “High-Resolution NMR Spectra With J Couplings in Solids”, Journal of Magnetic Resonance, 48, 524 (1982).
  18. Solum, M. S., Zilm, K. W., Michl, J., and Grant, D. M., “Carbon-13 Line Shape Study Of Two-Site Exchange in Solid Dimethyl Sulfone”, Journal of Physical Chemistry, 87, 2940 (1983).
  19. Zilm, K. W., Grant, D. M., Michl, J., Fink, M. J., and West, R., “Electronic-Structure of the Silicon Silicon Double-Bond: 29Si Shielding Anisotropy in Tetramesityldisilene”, Or-ganometallics, 2, 193 (1983).
  20. Alemany, L. B., Grant, D. M., Pugmire, R. J., Alger, T. D., and Zilm, K. W., “Cross Polarization and Magic Angle Sample Spinning NMR-Spectra of Model Organic Compounds I. Highly Protonated Molecules”, Journal of the American Chemical Society, 105, 2133 (1983).
  21. Alemany, L. B., Grant, D. M., Pugmire, R. J., Alger, T. D., and Zilm, K. W., “Cross Polarization and Magic Angle Sample Spinning NMR Spectra of Model Organic Com- pounds II. Molecules of Low Or Remote Protonation”, Journal of the American Chemical Society, 105, 2142 (1983).
  22. Duijvestijn, M. J., Vanderlugt, C., Smidt, J., Wind, R. A., Zilm, K. W., and Staplin, D. C., “13C NMR Spectroscopy in Diamonds Using Dynamic Nuclear Polarization”, Chemical Physics Letters, 102, 25 (1983).
  23. Strub, H., Beeler, A. J., Grant, D. M., Michl, J., Cutts, P. W., and Zilm, K. W., “Low- Temperature 13C Magnetic-Resonance in Solids II. 6p- Electron Ring-Systems - C7H7+, C6H6, and C5H5- “,Journal of the American Chemical Society, 105, 3333 (1983).
  24. Weitekamp, D. P.; Bielecki, A.; Zax, D.; Zilm, K. W.; and Pines, A., “Zero-Field NMR” Physical Review Letters, 50, 1807 (1983).
  25. Bielecki, A., Murdoch, J. B., Weitekamp, D. P., Zax, D. B., Zilm, K. W., Zimmermann, H., and Pines, A., “Fourier-Transform Pure Nuclear-Quadrupole Resonance By Pulsed Field Cycling”, Journal of Chemical Physics, 80, 2232 (1984).
  26. Lee, J. N., Alderman, D. W., Jin, J. Y., Zilm, K. W., Mayne, C. L., Pugmire, R. J., and Grant, D. M., “Cylindrical Spinner and Speed Controller For Magic Angle Spinning Nu- clear Magnetic-Resonance”, Review of Scientific Instruments, 55, 516 (1984).
  27. Beeler, A. J., Orendt, A. M., Grant, D. M., Cutts, P. W., Michl, J., Zilm, K. W., Downing, J. W., Facelli, J. C., Schindler, M. S., and Kutzelnigg, W., “Low-Temperature 13C Mag- netic-Resonance in Solids III. Linear and Pseudolinear Molecules”, Journal of the American Chemical Society, 106, 7672 (1984).
  28. Zax, D. B., Bielecki, A., Weitekamp, D. P., Zilm, K. W., and Pines, A., “Time Domain Zero Field Magnetic Resonance”, Proceedings of the XXIInd Congress Ampere on Magnetic Resonance and Related Phenomena Proceedings. Univ. Zurich, Zurich, Switzerland (1984).
  29. Zax, D. B., Bielecki, A., Zilm, K. W., and Pines, A., “Heteronuclear Zero-Field NMR”, Chemical Physics Letters, 106, 550 (1984).
  30. Zax, D. B., Bielecki, A., Zilm, K. W., Pines, A., and Weitekamp, D. P., “Zero field NMR
    and NQR”, Journal of Chemical Physics, 83, 4877 (1985).
  31. Mallouk, T., Hawkins, B.L., Conrad, M. P., Zilm, K. W., Maciel, G. E., and Bartlett, N., “Raman, Infrared and NMR Studies of the Graphite Hydrofluoride CxF1-5 (HF)5 2≤x≤5”,Philosophical Transactions of the Royal Society London, A 314,179 (1985).
  32. Zilm, K. W. and Webb, G. G., “13C Proton Shift Correlation Spectroscopy of a Whole Coal”, Fuel, 65, 721 (1986).
  33. Zilm, K. W., Merrill, R. A., Kummer, M. W., and Kubas, G. J., “Characterization of Transition-Metal Molecular-Hydrogen Complexes By Solid-State Proton NMR”, Journal of the American Chemical Society, 108, 7837 (1986).
  34. Bielecki, A., Zax, D. B., Zilm, K. W., and Pines, A., “Zero-field NMR and NQR spectrometer”, Review of Scientific Instruments, 57, 393 (1986).
  35. Zilm, K. W., Lawless, G. A., Merrill, R. M., Millar, J. M., and Webb, G. G., “Nature of the Tin-Tin Double-Bond as Studied By Solid-State and Solution Nuclear Magnetic Resonance”, Journal of the American Chemical Society, 109, 7236 (1987).
  36. Zilm, K. W., Merrill, R. A., Greenberg, M. M., and Berson, J. A., “The 1st Magic Angle Spinning NMR Spectrum of a Captive Intermediate: Direct Observation of a Singlet Ground-State Biradical, 3,4-Dimethylenefuran”, Journal of the American Chemical Society, 109, 1567 (1987).
  37. Zilm, K. W., Webb, G. G., Cowley, A. H., Pakulski, M., and Orendt, A., “The Nature of the Phosphorus-Phosphorus Double-Bond as Studied by Solid-State NMR”, Journal of the American Chemical Society, 110, 2032 (1988).
  38. Zilm, K. W., and Webb, G. G., “Applications of Zero-Field and Two-Dimensional NMR Methods to Fossil-Fuels”, Fuel, 67, 707 (1988).
  39. Webb, G. G., and Zilm, K. W., “Asynchronous MASSLF Spectroscopy - a Convenient Method For Assigning Solid-State 13C CPMAS Spectra”, Journal of the American Chemical Society, 111, 2455 (1989).
  40. Duncan, T. M., Zilm, K. W., Hamilton, D. M., and Root, T. W., “Adsorbed States of CO On Dispersed Metals - a High-Resolution Solid-State NMR Study”, Journal of Physical Chemistry, 93, 2583 (1989).
  41. Zilm, K. W., Heinekey, D. M., Millar, J. M., Payne, N. G., and Demou, P., “Proton Proton-Exchange Couplings in Transition-Metal Polyhydrides”, Journal of the American Chemical Society, 111, 3088 (1989).
  42. Zilm, K. W., Merrill, R. A., Webb, G. G., Greenberg, M. M., and Berson, J. A., “Two- Dimensional Solid-State NMR of a Captive Intermediate: Structure of the Radical Centers in 3,4-Dimethylenethiophene”, Journal of the American Chemical Society, 111, 1533 (1989).
  43. Zilm, K. W., Bonneviot, L., Hamilton, D. M., Webb, G. G., and Haller, G. L., “C-13 NMR-Studies of CO Adsorbed on Supported Platinum and Palladium Catalysts Using Magic Angle Sample Spinning”, Journal of Physical Chemistry, 94, 1463 (1990).
  44. Tycko, R., Dabbagh, G., Duchamp, J. C., and Zilm, K. W., “Carbon-13 Zero-Field NMR In High Field”, Journal of Magnetic Resonance, 89, 205 (1990).
  45. Duchamp, J. C., Pakulski, M., Cowley, A. H., and Zilm, K. W., “Nature of the Carbon Phosphorus Double-Bond and the Carbon Phosphorus Triple Bond As Studied By Solid- State NMR”, Journal of the American Chemical Society, 112, 6803 (1990).
  46. Heinekey, D. M., Millar, J. M., Koetzle, T. F., Payne, N. G., and Zilm, K. W., “Structural and Spectroscopic Characterization of Iridium Trihydride Complexes - Evidence For Proton-Proton Exchange Coupling”, Journal of the American Chemical Society, 112, 909 (1990).
  47. Zilm, K. W., Heinekey, D. M., Millar, J. M., Payne, N. G., Neshyba, S. P., Duchamp, J. C., and Szczyrba, J., “Quantum-Mechanical Exchange of Hydrides in Solution: Proton- Proton Exchange Couplings in Transition-Metal Polyhydrides”, Journal of the American Chemical Society, 112, 920 (1990).
  48. Zilm, K. W., Bonneviot, L., Haller, G. L., Han, O. H., and Kermarec, M., “13C NMR- Spectra of 13CO Adsorbed on Silica-Supported Palladium Particles: Particle-Size Dependence of the Surface Diffusion Rate and the 13C Knight-Shift”, Journal of Physical Chemistry, 94, 8495 (1990).
  49. Zilm, K. W.; Millar, J. M., “Solid State and Solution NMR of Non-Classical Transition Metal Polyhydrides” Advances in Magnetic and Optical Resonance, 15, 163-200 (1990).
  50. Greenberg, M. M., Blackstock, S. C., Berson, J. A., Merrill, R. A., Duchamp, J. C., and Zilm, K. W. “Structure of the Carrier of the Cross-Polarization Magic Angle Spinning 13C Nuclear-Magnetic-Resonance Signal Assigned to 3,4-Dimethylenethiophene - Multiple Position-Labeling and Chemical Trapping in Annealed Glasses” Journal of the American Chemical Society, 113, 2318 (1991).
  51. Wu, X. L., and Zilm, K. W., “Heterogeneity of Cross Relaxation in Solid-State NMR”, Journal of Magnetic Resonance, 93, 265 (1991).
  52. Reynolds, J. H., Berson, J. A., Kumashiro, K. K., Duchamp, J. C., Zilm, K. W., Rubello, A., and Vogel, P., “A Kinetically Stable Singlet-State of 1,2,4,5- Tetramethyleneben- zene”, Journal of the American Chemical Society, 114, 763 (1992).
  53. Inati, S. J., and Zilm, K. W., “Spin Correlations and Symmetrization in the Nuclear Magnetic Resonance of Molecular Systems with Tunneling”, Physical Review Letters, 68, 3273 (1992).
  54. Wu, X., and Zilm, K. W., “Cross Polarization with High Speed Magic Angle Spinning”, Journal of Magnetic Resonance Series A, 104, 154 (1993).
  55. Wisniewski, L. L., Mediati, M., Jensen, C. M., and Zilm, K. W., “Mechanism of Hydride Scrambling in a Transition-Metal Dihydrogen Dihydride as Studied by Solid-State Proton NMR”, Journal of the American Chemical Society, 115, 7533 (1993).
  56. Han, O. H., Lin, C. Y., Sustache, N., McMillan, M., Carruthers, J. D., Zilm, K. W., and Haller, G. L., “Solid State Nuclear Magnetic Resonance Spectroscopic Investigation of Hydrotreating Catalysts and Related Materials”, Applied Catalysis A-General, 98, 195 (1993).
  57. Han, O. H., Larsen, G., Zilm, K. W., and Haller, G. L., “Methoxy Formation Spillover on Pd/Al2O3 Studied By C-13,H-1 NMR”, Studies in Surface Science and Catalysis, 77, 223 (1993).
  58. Maitre, P., Eisenstein, O., Michos, D., Luo, X. L., Siedle, A. R., Wisnieski, L., Zilm, K.W., and Crabtree, R. H., “B11H14 (-)- a Nido Cage With No H…H Interaction”, Journal of the American Chemical Society, 115, 7747 (1993).
  59. Wu, X.L., and Zilm, K.W., “Complete Spectral Editing in CPMAS NMR”. Journal of Magnetic Resonance Series A, 102, 205 (1993).
  60. Augustine, M. P., Zilm, K. W., and Zax, D. B., “Field Dependent Isotropic Shifts in Solid State Nuclear Magnetic Resonance: a Floquet Treatment”, Journal of Chemical Physics, 98, 9432 (1993).
  61. Reynolds, J. H., Berson, J. A., Kumashiro, K. K., Duchamp, J. C., Zilm, K. W., Scaiano, J. C., Berinstain, A. B., Rubello, A., and Vogel, P., “2,3,5,6-Tetrakis(Methylene)-1,4- Cyclohexanediyl (1,2,4,5- Tetramethylenebenzene), a Disjoint Non-Kekule Singlet Hydrocarbon Biradical”, Journal of the American Chemical Society, 115, 8073 (1993).
  62. Cavalieri, J. D., West, R., Duchamp, J. C., and Zilm, K. W., “Unusual 29Si Chemical- Shift Anisotropies in 3-Membered Rings”, Journal of the American Chemical Society, 115, 3770 (1993).
  63. Wu, X. L., and Zilm, K. W., “Methylene-Only Subspectrum in CPMAS NMR”, Journal of Magnetic Resonance Series A, 104, 119 (1993).
  64. Zilm, K. W.; Duchamp, J. C.,”Comparisons of Shielding Anisotropies for Different Nu- clei and Other Insights Into Shielding From an Experimentalist’s Viewpoint” NATO ASI Series C, Vol. 386, pg.315-334 (1993) “Nuclear Magnetic Shieldings and Molecular Structure” ed. J. Tossel, Kluwer Academic Pub.
  65. West, R., Cavalieri, J. D., Duchamp, J., and Zilm, K. W., “Chemical-Shift Tensors and Chemical Bonding in Cyclic Silanes”, Phosphorus Sulfur and Silicon and the Related Elements, 93, 213 (1994).
  66. Arduengo, A. J., Dixon, D. A., Kumashiro, K. K., Lee, C., Power, W. P., and Zilm, K. W., “Chemical Shielding Tensor of a Carbene”, Journal of the American Chemical Society, 116, 6361 (1994).
  67. Xiaoling, W., Burns, S. T., and Zilm, K. W., “Spectral Editing in CPMAS NMR. Generating Subspectra Based on Proton Multiplicities”, Journal of Magnetic Resonance, Series A, 111, 29 (1994).
  68. Regnier, P., Lasaga, A. C., Berner, R. A., Han, O. H., and Zilm, K. W., “Mechanism of (CO3)2- Substitution in Carbonate-Fluorapatite - Evidence From FTIR Spectroscopy, C- 13 NMR, and Quantum- Mechanical Calculations”, American Mineralogist, 79, 809 (1994).
  69. Kubas, G. J., Nelson, J.E.; Bryan, J.C.; Eckert, J.; Wisniewski, L.; Zilm, K.W. “Isolation of an Extremely Labile Dihydrogen Complex, Cr(CO)3PPr13(H2), Containing the Shortest Ligated H-H Bond” Inorganic Chemistry, 33, 2954-2960 (1994).
  70. Zilm, K.W. “Quantum Exchange” Encyclopedia of Nuclear Magnetic Resonance, John Wiley and Sons Ltd., 3916-3925(1995).
  71. Zilm, K.W. “Spectral Editing in 13C Spectra of Hydrocarbon Solids” Encyclopedia of Nuclear Magnetic Resonance, John Wiley and Sons Ltd., 4498-4504 (1995).
  72. King, W. A., Luo, X. L., Scott, B. L., Kubas, G. J., and Zilm, K. W., “Cationic Manga- nese(I) Dihydrogen and Dinitrogen Complexes Derived From A Formally 16-Electron Complex With A Bis-Agostic Interaction, [Mn(CO)(Ph2PC2H4PPh2)2]+”, Journal of the American Chemical Society, 118, 6782 (1996).
  73. Augustine, M. P., and Zilm, K. W., “Observation Of Bulk Susceptibility Effects In High- Resolution Nuclear Magnetic Resonance”, Journal of Magnetic Resonance Series A, 123, 145 (1996).
  74. Augustine, M. P., and Zilm, K. W., “Optical Pumping Magnetic Resonance in High Magnetic Fields: Characterization Of Nuclear Relaxation During Pumping”, Journal of Chemical Physics, 105, 2998 (1996).
  75. Augustine, M. P., and Zilm, K. W., “Optical Pumping Magnetic Resonance in High Magnetic Fields: Characterization of The Optical Properties of Rb-Xe Mixtures”, Molecular Physics, 89, 737 (1996).
  76. Augustine, M. P., and Zilm, K. W., “Optical Pumping Magnetic Resonance in High Magnetic Fields: Measurement of High Field Spin Exchange Cross Sections”, Chemical Physics Letters, 280, 1 (1997).
  77. West, R., Cavalieri, J. D., Buffy, J. J., Fry, C., Zilm, K. W., Duchamp, J. C., Kira, M., Iwamoto, T., Muller, T., and Apeloig, Y., “A Solid State NMR and Theoretical Study of the Chemical Bonding in Disilenes”, Journal of the American Chemical Society, 119, 4972 (1997).
  78. Wiberg, K. B.; Hammer, J. D.; Keith, T.A.; Zilm, K. W. “13C NMR Chemical Shifts of Methyl Cation and Anion: A Relationship Between Chemical Shift and Charge” Tetrahedron Letters, 38, 323-326 (1997).
  79. Han, O. H., Larsen, G., Haller, G. L., and Zilm, K. W., “Carbon-13 Nuclear Magnetic Resonance Spectroscopic Studies of 13CO Adsorbed on Platinum Particles in L-Zeolites”, Bulletin of the Korean Chemical Society, 19, 934 (1998).
  80. Han, O. H., Haller, G. L., and Zilm, K. W., “Reconstruction of Pd Particles Supported on Silica in The Presence of CO as Studied by Carbon-13 NMR”, Bulletin of the Korean Chemical Society, 19, 942 (1998).
  81. Wiberg, K. B., Hammer, J. D., Zilm, K. W., Cheeseman, J. R., and Keith, T. A., “NMR Chemical Shifts. 1. The Role Of Relative Atomic Orbital Phase In Determining The Sign Of The Paramagnetic Terms: ClF, CH3F, CH3NH3+, FNH3+, and HC=CF”, Journal of Physical Chemistry A, 102, 8766 (1998).
  82. Wiberg, K.B., J.D. Hammer, T.A. Keith, and K. Zilm, “NMR chemical shifts. 2. Interpre- tation of the Carbon Chemical Shifts in Monocyclic Aromatic Compounds and Carbenes”, Journal of Physical Chemistry A,  103, 21-27 (1999).
  83. Wiberg, K.B., J.D. Hammer, K.W. Zilm, and J.R. Cheeseman, “NMR Chemical Shifts. 3. A Comparison of Acetylene, Allene, and the Higher Cumulenes”, Journal of Organic Chemistry,  64, 6394-6400 (1999).
  84. Burns, S.T., X.L. Wu, and K.W. Zilm, “Improvement of Spectral Editing in Solids: A Sequence for Obtaining 13CH + 13CH2 -only 13C Spectra”, Journal of Magnetic Resonance, 143, 352-359 (2000).
  85. McDermott, A., T. Polenova, A. Bockmann, K.W. Zilm, E.K. Paulson, R.W. Martin, and G.T. Montelione, “Partial NMR Assignments for Uniformly (C-13, N-15)-Enriched BPTI in the Solid State”, Journal of Biomolecular NMR, 16, 209-219 (2000).
  86. Wiberg, K.B. and K.W. Zilm, “F-19 NMR chemical shifts. 1. Aliphatic fluorides”, Journal of Organic Chemistry, 66, 2809-2817 (2001).
  87. Lupták, A., Ferré-D’Amaré, A. R., Zhou, K., Zilm, K.W., and Doudna, J.A. “Direct pKa Measurement of the Active Site Cytosine in a Genomic HDV Ribozyme”, Journal of the American Chemical Society, 123, 8447-8452 (2001).
  88. Martin, R. W., Paulson, E. K., Zilm, K. W. “Design of a Triple Resonance MAS Probe for High Field Solid State NMR”, Review of Scientific Instruments, 74, 1-17 (2003)
  89. Martin, R.W.. Paulson, E.,K.,Zilm, K.W. ” Design of a Triple Resonance MAS Probe for High Field Solid State NMR”, Review of Scientific Instruments, 74, 1-17 (2003). 
  90. Morcombe, C. R., Zilm, K. W. “Chemical Shift Referencing in MAS Solid State NMR”, Journal of Magnetic Resonance, 162, 173-180 (2003).
  91. Martin, R.W., Zilm, K. W. “Protein Nanocrystals and their Characterization by Solid State NMR” Journal of Magnetic Resonance, 165, 162-174 (2003).
  92. Gehman, J. D., Paulson, E. K., and Zilm, K. W. “The influence of internuclear spatial distribution and instrument noise on the precision of distances determined by solid state NMR of isotopically enriched proteins” Journal of Biomolecular NMR, 27,235-259 (2003).
  93. Paulson, E. K., Morcombe, C. R., Gaponenko, V., Dancheck, B., Byrd, R.A., Zilm, K. W. “High Sensitivity Observation of Dipolar Exchange and NOEs Between Exchangeable Protons in Proteins by 3D Solid State NMR Spectroscopy”, Journal of the American Chemical Society, 125,14222-14223 (2003).
  94. Paulson, E. K., Morcombe, C. R., Gaponenko, V., Dancheck, B., Byrd, R.A., Zilm, K. W. “Sensitive High Resolution Inverse Detection NMR Spectroscopy of Proteins in the Solid State”, Journal of the American Chemical Society, 125, 15831-15836 (2003).
  95. Martin, R. W. and Zilm, K. W., “Variable Temperature System Using Vortex Tube Cool- ing and Fiber Optic Temperature Measurement for Low Temperature Magic Angle Spin- ning NMR”, Journal of Magnetic Resonance, 168, 202-209 (2004).
  96. Wiberg, K. B., Hammer, J. D., Zilm, K. W., Keith, T. A., Cheeseman, J. R., Duchamp, J. C., “NMR Chemical Shifts. Substituted Acetylenes”, Journal of Organic Chemistry, 69, 1086-1096 (2004).
  97. Paulson, E.K. and Zilm, K. W. “Linear Phase Correction of Folded Multidimensional NMR Data by Zero Inter-filling”, Journal of Magnetic Resonance, 168, 217-219 (2004).
  98. Igumenova, T. I., McDermott, A. E., Zilm, K.W., Martin, R. W., Paulson, E. K., Wand, A.  J. “Assignments of Carbon Resonances for Microcrystalline Ubiquitin” Journal of the American Chemical Society, 126, 6720-6727 (2004).
  99. Morcombe, C. R., Gaponenko, V., Byrd, R. A., Zilm, K. W. “Diluting Abundant Spins by Isotope Edited Radio Frequency Field Assisted Diffusion” Journal of the American Chemical Society, 126, 7196-7197 (2004).
  100. Paulson, E.K., Martin, R. W., and Zilm, K. W. “RF Homogeneity in High Field Solid State NMR Probes”, 171, 314-323, Journal of Magnetic Resonance, (2004).
  101. Morcombe, E. K., Gaponenko, V., Byrd, R. A., Zilm, K. W. “13C CPMAS Spectroscopy of Deuterated Proteins: CP Dynamics, Line Shapes and T1 Relaxation”, Journal of the American Chemical Society, 127, 397-404 (2005).
  102. Paulson, E.K. and Zilm, K.W. “External Field Frequency Lock Probe for High Resolution Solid State NMR”, Review of Scientific Instruments, 76, article 026104 (2005).
  103. Morcombe, C. R., Paulson, E. K., Gaponenko, V., Byrd, R. A., Zilm, K. W. “1H-15N Correlation Spectroscopy in Nanocrystalline Proteins”, Journal of Biomolecular NMR, 31, 217-230 (2005).
  104. Harris, R. K., Becker, E.D., Cabral De Menezes, S. M., Granger, P., Hoffman, R. E., and Zilm, K. W. “Further Conventions For NMR Shielding and Chemical Shifts”, Pure Appl. Chem., 80, 59–84 (2008).
  105. Fry, E.A., Sengupta, S, Phan„ V.C., Kuang, S. and Kurt W. Zilm, K.W. “CSA Enabled Spin Diffusion leads to MAS Rate Dependent T1’s at high field” accepted for publication, Journal of the American Chemical Society, (2010).